C₁₆H₁₀⁽²⁾H₉BrN₂

Base Information

Chemical Name:C₁₆H₁₀⁽²⁾H₉BrN₂
CAS No.:1287739-34-7
Molecular Formula:C₁₆H₁₉BrN₂
Molecular Weight:328.173
Hs Code.:

C<sub>16</sub>H<sub>10</sub><sup>(2)</sup>H<sub>9</sub>BrN<sub>2</sub>

Synonyms:C₁₆H₁₀⁽²⁾H₉BrN₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₀⁽²⁾H₉BrN₂

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Technology Process of C₁₆H₁₀⁽²⁾H₉BrN₂

There total 7 articles about C₁₆H₁₀⁽²⁾H₉BrN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1287739-30-3
N-(3-bromophenyl-4-tert-butyl-d9)-2-nitroaniline

: 1287739-34-7
C₁₆H₁₀⁽²⁾H₉BrN₂

Guidance literature:: With hydrogenchloride; ammonium chloride; iron; In ethanol; water; at 50 - 70 ℃; for 3h;

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 1287739-34-7
C₁₆H₁₀⁽²⁾H₉BrN₂

Guidance literature:: Multi-step reaction with 7 steps

1: iron(III) chloride / 22 - 25 °C

2: nitric acid; sulfuric acid / water / 20 °C

3: hydrogen / 20 % Pd(OH)2/C / methanol / 3 h / 2585.81 Torr

4: nitric acid / water / 20 °C

5: sulfuric acid / water / 8 h / 20 - 100 °C

6: sodium t-butanolate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 5 h / 100 °C / Inert atmosphere; Sealed tube

7: hydrogenchloride; ammonium chloride / iron / ethanol; water / 3 h / 50 - 70 °C

With hydrogenchloride; iron(III) chloride; sulfuric acid; hydrogen; nitric acid; ammonium chloride; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 20 % Pd(OH)2/C; iron; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In methanol; ethanol; water; toluene;

Reference yield:

: 1287739-17-6
1-tert-butyl-4-nitrobenzene

: 1287739-34-7
C₁₆H₁₀⁽²⁾H₉BrN₂

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / 20 % Pd(OH)2/C / methanol / 3 h / 2585.81 Torr

2: nitric acid / water / 20 °C

3: sulfuric acid / water / 8 h / 20 - 100 °C

4: sodium t-butanolate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 5 h / 100 °C / Inert atmosphere; Sealed tube

5: hydrogenchloride; ammonium chloride / iron / ethanol; water / 3 h / 50 - 70 °C

With hydrogenchloride; sulfuric acid; hydrogen; nitric acid; ammonium chloride; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 20 % Pd(OH)2/C; iron; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In methanol; ethanol; water; toluene;