(2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

Base Information

Chemical Name:(2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate
CAS No.:1195788-02-3
Molecular Formula:C₃₅H₅₀O₈Si
Molecular Weight:626.863
Hs Code.:

Synonyms:(2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

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Chemical Property of (2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

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Technology Process of (2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

There total 1 articles about (2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 264132-64-1
C₂₃H₄₀O₂Sn

: 1195788-01-2
(2R,3R,5R,E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-7-iodohept-6-ene-2,3-diyl diacetate

: 1195788-02-3
(2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jo901793f

Reference yield: 86.0%

: 1195788-02-3
(2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

: 1195788-03-4
(2R,3R,5R,6E,8E)-1-benzyloxy-5-hydroxy-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate

Guidance literature:: (2R,3R,5R,6E,8E)-1-benzyloxy-5-(tert-butyldimethylsilyloxy)-10-(4-methoxybenzyloxy)deca-6,8-diene-2,3-diyl diacetate; With pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 35 ℃;

With water; sodium hydrogencarbonate; In tetrahydrofuran;
DOI:10.1021/jo901793f