benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

Base Information

Chemical Name:benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate
CAS No.:1311569-04-6
Molecular Formula:C₂₉H₄₁N₃O₆
Molecular Weight:527.661
Hs Code.:

Synonyms:benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

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Chemical Property of benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

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Technology Process of benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

There total 5 articles about benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1311569-03-5
benzyl 3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)-4-nitrobenzoate

: 1311569-04-6
benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

Guidance literature:: With acetic acid; zinc; In methanol; for 0.333333h;

Reference yield:

: 157665-51-5
3-fluoro-4-nitrobenzoyl chloride

: 1311569-04-6
benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 16 h

2: potassium carbonate / acetonitrile / 16 h / 80 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C

4: zinc; acetic acid / methanol / 0.33 h

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; acetic acid; triphenylphosphine; zinc; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;

Reference yield:

: 403-21-4
3-fluoro-4-nitrobenzoic acid

: 1311569-04-6
benzyl 4-amino-3-({4-[bis(tert-butoxycarbonyl)amino]-2-methylbutan-2-yl}amino)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

2: pyridine / dichloromethane / 16 h

3: potassium carbonate / acetonitrile / 16 h / 80 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C

5: zinc; acetic acid / methanol / 0.33 h

With pyridine; oxalyl dichloride; di-isopropyl azodicarboxylate; potassium carbonate; acetic acid; triphenylphosphine; zinc; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;