methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside
CAS No.:716329-02-1
Molecular Formula:C₁₆H₂₀N₄O₅
Molecular Weight:348.359
Hs Code.:

Synonyms:methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

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Chemical Property of methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

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Technology Process of methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

There total 3 articles about methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 716329-01-0
methyl 2-acetamido-3-O-benzoyl-2,6-dideoxy-α-D-glucopyranoside

: 716329-02-1
methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

Guidance literature:: With diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1081/CAR-120030468

Reference yield:

: 87236-56-4
methyl 2-acetamido-6-bromo-2,6-dideoxy-α-D-glucopyranoside

: 716329-02-1
methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / methanol / 48 h / 20 °C / 760 Torr

2: 89 percent / pyridine / 5 h / -35 - 20 °C

3: 92 percent / PPh₃; DEAD; (PhO)2PON₃ / tetrahydrofuran / 24 h / 20 °C

With pyridine; diphenyl phosphoryl azide; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methanol; 3: Mitsunobu reaction;
DOI:10.1081/CAR-120030468

Reference yield:

: 50286-18-5
methyl 2-acetamido-2,6-dideoxy-α-D-glucopyranoside

: 716329-02-1
methyl 2-acetamido-4-azido-3-O-benzoyl-2,4,6-trideoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 5 h / -35 - 20 °C

2: 92 percent / PPh₃; DEAD; (PhO)2PON₃ / tetrahydrofuran / 24 h / 20 °C

With pyridine; diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1081/CAR-120030468