[Rh((borane)(NMe₂BH₂)(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

Base Information

Chemical Name:[Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]
CAS No.:1192372-95-4
Molecular Formula:C₂₈H₇₂B₂N₂P₂Rh*C₃₂H₁₂BF₂₄
Molecular Weight:1486.59
Hs Code.:

[Rh((borane)*(NMe<sub>2</sub>BH<sub>2</sub>)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4]

Synonyms:[Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

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Chemical Property of [Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

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Technology Process of [Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

There total 3 articles about [Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 21793-61-3
dimethylamine-dimethylaminoborane-borane

: 1073349-09-3
[Rh(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

: 1192372-95-4
[Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

Guidance literature:: In further solvent(s); (Ar), Schlenk techniques; addn. of boron compd. to soln. of rhodium complex in 1,2-F2C6H4; diffusion of pentane at -35°C, isolation of crystals;
DOI:10.1021/ja906070r

Reference yield:

: 21793-61-3
dimethylamine-dimethylaminoborane-borane

: 1192372-91-0
[Rh(η6-1,2-F2C6H4)(P(i-Bu)3)2][B(3,5-C6H3(CF3)2)4]

: 1192372-95-4
[Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

Guidance literature:: In further solvent(s); (Ar), Schlenk techniques; addn. of boron compd. to soln. of rhodium complex in 1,2-F2C6H4;
DOI:10.1021/ja906070r

Reference yield:

: 21793-61-3
dimethylamine-dimethylaminoborane-borane

: 1073349-09-3
[Rh(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

: 1073349-16-2
[Rh(H)2((borane)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

: 1192372-97-6
[Rh(H)2((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

: 1192372-95-4
[Rh((borane)*(NMe₂BH₂)*(dimethylamine))(P(i-Bu)3)2][B(3,5-C₆H₃(CF₃)2)4]

Guidance literature:: In further solvent(s); (Ar), Schlenk techniques; addn. of soln. of boron compd. (2 equiv.) in 1,2-F2C6H4 to soln. of rhodium complex in 1,2-F2C6H4; not isolated, NMR;
DOI:10.1021/ja906070r