Technology Process of 9-(2-hydroxyphenyl)anthracene triflate
There total 6 articles about 9-(2-hydroxyphenyl)anthracene triflate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
dichloromethane;
at -30 - 0 ℃;
for 1h;
DOI:10.1021/jo00058a023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) BuLi, 2) MgBr2 / 1) ether, hexane, RT, 3 h
2: <1,2-bis(diphenylphosphino)ethane>nickel (II) chloride / tetrahydrofuran / 1) -78 deg C, to RT, 2) reflux, overnight
3: 86 percent / 4N HCl / tetrahydrofuran / 3 h / Heating
4: 96 percent / 2,6-lutidine / CH2Cl2 / 1 h / -30 - 0 °C
With
2,6-dimethylpyridine; hydrogenchloride; n-butyllithium; magnesium bromide;
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00058a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: <1,2-bis(diphenylphosphino)ethane>nickel (II) chloride / tetrahydrofuran / 1) -78 deg C, to RT, 2) reflux, overnight
2: 86 percent / 4N HCl / tetrahydrofuran / 3 h / Heating
3: 96 percent / 2,6-lutidine / CH2Cl2 / 1 h / -30 - 0 °C
With
2,6-dimethylpyridine; hydrogenchloride;
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00058a023
