C₃₇H₃₅O₁₂P

Base Information

Chemical Name:C₃₇H₃₅O₁₂P
CAS No.:363619-65-2
Molecular Formula:C₃₇H₃₅O₁₂P
Molecular Weight:702.651
Hs Code.:

C<sub>37</sub>H<sub>35</sub>O<sub>12</sub>P

Synonyms:C₃₇H₃₅O₁₂P

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Chemical Property of C₃₇H₃₅O₁₂P

Chemical Property:

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Technology Process of C₃₇H₃₅O₁₂P

There total 12 articles about C₃₇H₃₅O₁₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41308-76-3,821794-45-0
allyl α-D-mannopyranoside

: 363619-65-2
C₃₇H₃₅O₁₂P

Guidance literature:: Multi-step reaction with 6 steps

1.1: 90 percent / TsOH*H₂O / acetone

2.1: AcOH; H₂O / 12 h / 0 °C

3.1: NaH / dimethylformamide / 2 h

4.1: KOBu-t / dimethylsulfoxide / 1 h / 60 °C

4.2: Hg(OAc)2 / tetrahydrofuran; H₂O / 0.33 h

5.1: 85 percent / LiHMDS / tetrahydrofuran / 55 °C

6.1: H₂ / Pd(OH)2/C / methanol

6.2: Dowex-50 (H(+)) / methanol

6.3: DMAP / pyridine

With potassium tert-butylate; water; hydrogen; sodium hydride; acetic acid; lithium hexamethyldisilazane; palladium dihydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)00961-3

Reference yield:

: 119111-31-8
allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 363619-65-2
C₃₇H₃₅O₁₂P

Guidance literature:: Multi-step reaction with 7 steps

1.1: 94 percent / MeONa / methanol

2.1: 90 percent / TsOH*H₂O / acetone

3.1: AcOH; H₂O / 12 h / 0 °C

4.1: NaH / dimethylformamide / 2 h

5.1: KOBu-t / dimethylsulfoxide / 1 h / 60 °C

5.2: Hg(OAc)2 / tetrahydrofuran; H₂O / 0.33 h

6.1: 85 percent / LiHMDS / tetrahydrofuran / 55 °C

7.1: H₂ / Pd(OH)2/C / methanol

7.2: Dowex-50 (H(+)) / methanol

7.3: DMAP / pyridine

With potassium tert-butylate; water; hydrogen; sodium hydride; acetic acid; lithium hexamethyldisilazane; palladium dihydroxide; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)00961-3

Reference yield:

: 85207-15-4
allyl 2,3:4,6-di-O-isopropylidene-α-D-mannopyranoside

: 363619-65-2
C₃₇H₃₅O₁₂P

Guidance literature:: Multi-step reaction with 5 steps

1.1: AcOH; H₂O / 12 h / 0 °C

2.1: NaH / dimethylformamide / 2 h

3.1: KOBu-t / dimethylsulfoxide / 1 h / 60 °C

3.2: Hg(OAc)2 / tetrahydrofuran; H₂O / 0.33 h

4.1: 85 percent / LiHMDS / tetrahydrofuran / 55 °C

5.1: H₂ / Pd(OH)2/C / methanol

5.2: Dowex-50 (H(+)) / methanol

5.3: DMAP / pyridine

With potassium tert-butylate; water; hydrogen; sodium hydride; acetic acid; lithium hexamethyldisilazane; palladium dihydroxide; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)00961-3