1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea

Base Information

• Chemical Name: 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea
• CAS No.: 1220124-75-3
• Molecular Formula: C₂₁H₂₄BrN₃O₂S
• Molecular Weight: 462.41

Synonyms:1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea

Chemical Property of 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea

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Technology Process of 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea

There total 2 articles about 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-bromophenyl isothiocyanate (2131-59-1) + C14H20N2O2 (950919-65-0) → 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)thiourea (1220124-75-3)

Guidance literature:

In acetonitrile; for 6h; Reflux;

DOI:10.1007/s12272-010-2223-9

Reference yield:

1,7,8,9,10-pentamethyl-4-azatricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (261160-84-3) → 1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)thiourea (1220124-75-3)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate

2: acetonitrile / 6 h / Reflux

With hydrazine hydrate; In acetonitrile;

DOI:10.1007/s12272-010-2223-9

Reference yield: 72.0%

1-(3-bromophenyl)-3-(1,7,8,9,10-pentamethyl-3,5-dioxo-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)thiourea (1220124-75-3) + water (7732-18-5) + copper dichloride → C42H46Br2CuN6O4S2*H2O

Guidance literature:

In N,N-dimethyl-formamide; at 23 ℃; for 1h;

DOI:10.1016/j.jinorgbio.2020.111234

upstream raw materials:

3-bromophenyl isothiocyanate

C₁₄H₂₀N₂O₂

1,7,8,9,10-pentamethyl-4-azatricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

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