C₅₄H₆₆N₈O₇

Base Information

Chemical Name:C₅₄H₆₆N₈O₇
CAS No.:1612853-92-5
Molecular Formula:C₅₄H₆₆N₈O₇
Molecular Weight:939.167
Hs Code.:

C<sub>54</sub>H<sub>66</sub>N<sub>8</sub>O<sub>7</sub>

Synonyms:C₅₄H₆₆N₈O₇

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Chemical Property of C₅₄H₆₆N₈O₇

Chemical Property:

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Technology Process of C₅₄H₆₆N₈O₇

There total 20 articles about C₅₄H₆₆N₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 1612853-91-4
C₂₇H₃₉BN₄O₆

: 1419387-22-6
C₃₄H₃₉F₃N₄O₆S

: 1612853-92-5
C₅₄H₆₆N₈O₇

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 4h; Inert atmosphere;

Reference yield:

: 1357259-32-5
C₁₃H₁₇BrN₂O₄S

: 1612853-92-5
C₅₄H₆₆N₈O₇

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

2: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 1 h / 20 °C

3: iron; ammonium chloride / water; methanol / 3 h / Reflux

4: acetic acid / 0.5 h / 80 °C

5: hydrogenchloride / ethyl acetate / 8 h / 20 °C

6: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C

7: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere

8: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; iron; potassium carbonate; ammonium chloride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1357259-36-9
C₁₉H₂₄BrN₃O₃

: 1612853-92-5
C₅₄H₆₆N₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / ethyl acetate / 8 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere

4: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;