(1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine

Base Information

• Chemical Name: (1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine
• CAS No.: 1034102-32-3
• Molecular Formula: C₄₂H₅₃NO₅Si
• Molecular Weight: 679.972

Synonyms:(1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine

Chemical Property of (1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine

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Technology Process of (1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine

There total 1 articles about (1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[(2S,3R,4S)-3,4-dibenzyloxy-2-pyrrolidinyl]-(1S,2S,3R)-1,2-dibenzyloxy-4-(tert-butyldimethylsilyloxy)-butan-3-ol (1034102-31-2) → (1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine (1034102-32-3) + C42H53NO5Si

Guidance literature:

With pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; at 20 ℃; for 72h;

DOI:10.1021/ol8009144

Reference yield:

(1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-3-((tert-butyldimethylsilyloxy)methyl)-hexahydro-1H-pyrrolizine (1034102-32-3) → ((1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-hexahydro-1H-pyrrolizin-3-yl)methanol (1034102-33-4)

Guidance literature:

With hydrogenchloride; water; In methanol; at 20 ℃; for 5h;

DOI:10.1021/ol8009144

upstream raw materials:

1-[(2S,3R,4S)-3,4-dibenzyloxy-2-pyrrolidinyl]-(1S,2S,3R)-1,2-dibenzyloxy-4-(tert-butyldimethylsilyloxy)-butan-3-ol

Downstream raw materials:

((1S,2S,3S,6S,7R,7aS)-1,2,6,7-tetrabenzyloxy-hexahydro-1H-pyrrolizin-3-yl)methanol

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