3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid

Base Information

• Chemical Name: 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid
• CAS No.: 25886-96-8
• Molecular Formula: C₁₆H₁₇I₃N₂O₆
• Molecular Weight: 714.034
• Mol file: 25886-96-8.mol

Synonyms:3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid

Chemical Property of 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid

There total 6 articles about 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodoglutaranilic acid (25883-00-5) → 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid (25886-96-8)

Guidance literature:

With dimethyl sulfate; In sodium hydroxide; ethyl acetate;

Reference yield:

3-Amino-2,4,6-triiodo-5-(N-methylacetamido)-benzoic acid (1949-42-4) → 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid (25886-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂SO₄, (ii) aq. NaOH

2: sodium hydroxide / acetone

With sodium hydroxide; In acetone;

Reference yield:

glutaric anhydride, (108-55-4) → 3'-carboxy-5'-(N-methylacetamido)-2',4',6'-triiodo-N-methylglutaranilic acid (25886-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂SO₄, (ii) aq. NaOH

2: sodium hydroxide / acetone

With sodium hydroxide; In acetone;

upstream raw materials:

glutaric anhydride,

3-Amino-2,4,6-triiodo-5-(N-methylacetamido)-benzoic acid

3-(acetyl-methyl-amino)-5-(2,6-dioxo-piperidin-1-yl)-2,4,6-triiodo-benzoic acid

methyl 4-(chlorocarbonyl)butyrate