1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

Base Information

Chemical Name:1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate
CAS No.:111512-73-3
Molecular Formula:C₂HF₃O₂*C₃₂H₄₀N₂O₂
Molecular Weight:598.706
Hs Code.:

1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzo<g>phthalazine trifluoroacetate

Synonyms:1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

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Chemical Property of 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

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Technology Process of 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

There total 5 articles about 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 111534-91-9
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

: 111512-73-3
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

Guidance literature:: With air; In diethyl ether; for 1h; Ambient temperature;

Reference yield:

: 111512-68-6
3,5-di-tert-butyl-4-oxo-3',6'-dimethyl-7'-(3'',5''-di-tert-butyl-4''-hydroxyphenyl)spiro<2,5-cyclohexadiene-1,1'-cyclopentapyridazine>

: 111512-73-3
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 12 h / Ambient temperature

2: 90 percent / air / diethyl ether / 1 h / Ambient temperature

With air; In diethyl ether;

Reference yield:

: 111534-90-8
3,4-Di(3,5-di-tert-butyl-5-hydroxybenzylidene)hexane-2,5-dione

: 111512-73-3
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)benzophthalazine trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / hydrazine hydrate / ethanol / 0.5 h / 80 °C

2: 78 percent / 12 h / Ambient temperature

3: 90 percent / air / diethyl ether / 1 h / Ambient temperature

With air; hydrazine hydrate; In diethyl ether; ethanol;