(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

Base Information

Chemical Name:(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide
CAS No.:68098-76-0
Molecular Formula:C₄₈H₆₆N₈O₁₄S₂
Molecular Weight:1043.23
Hs Code.:

(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)<SUB>2 </SUB>(serinehydroxy)-dilactone disulfide

Synonyms:(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

Chemical Property:

Purity/Quality:

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Technology Process of (N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

There total 3 articles about (N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₃H₇₆N₈O₁₇S₂

: 68098-76-0
(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃CO₂H

2: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl; N-hydroxybenzotriazole / CH₂Cl₂ / 24 h / 0 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2003.09.086

Reference yield:

: C₄₈H₆₈N₈O₁₅S₂

: 68098-76-0
(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1016/j.bmcl.2003.09.086

Reference yield:

: Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala-Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

: 68098-76-0
(N-Cbz-D-Ser-L-Ala-N-Me-L-Cys-N-Me-L-Val)₂(serinehydroxy)-dilactone disulfide

Guidance literature:: Multi-step reaction with 3 steps

1: I₂; methanol / CH₂Cl₂ / 25 °C

2: CF₃CO₂H

3: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl; N-hydroxybenzotriazole / CH₂Cl₂ / 24 h / 0 °C

With methanol; iodine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2003.09.086