1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester
CAS No.:853070-96-9
Molecular Formula:C₂₂H₁₄Cl₂O₅
Molecular Weight:429.256
Hs Code.:

Synonyms:1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

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Chemical Property of 1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

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Technology Process of 1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

There total 7 articles about 1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 853070-72-1
1-trifluoromethanesulfonyloxydibenzofuran-4,6-dicarboxylic acid dimethyl ester

: 67492-50-6
(3,5-dichlorophenyl)boronic acid

: 853070-96-9
1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In methanol; toluene; for 12h; Heating;
DOI:10.1021/ja044351f

Reference yield:

: 853070-69-6
(dibenzofuran-1-yloxy)triisopropylsilane

: 853070-96-9
1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: sec-butyllithium; TMEDA / diethyl ether; cyclohexane / -78 - 20 °C

1.2: diethyl ether; cyclohexane / 0.5 h / -78 °C

2.1: 0.36 g / methanol; benzene; hexane

3.1: 97 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

4.1: 92 percent / pyridine / 0 - 20 °C

5.1: 52 percent / Pd(PPh₃)4; LiCl; aq. Na₂CO₃ / toluene; methanol / 12 h / Heating

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N,N,N,-tetramethylethylenediamine; tetrabutyl ammonium fluoride; sec.-butyllithium; sodium carbonate; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; cyclohexane; toluene; benzene; 5.1: Suzuki coupling;
DOI:10.1021/ja044351f

Reference yield:

: 853070-71-0
1-hydroxydibenzofuran-4,6-dicarboxylic acid dimethyl ester

: 853070-96-9
1-(3,5-dichlorophenyl)dibenzofuran-4,6-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 0 - 20 °C

2: 52 percent / Pd(PPh₃)4; LiCl; aq. Na₂CO₃ / toluene; methanol / 12 h / Heating

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In methanol; toluene; 2: Suzuki coupling;
DOI:10.1021/ja044351f