Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI)

Base Information

Chemical Name:Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI)
CAS No.:88155-16-2
Molecular Formula:C₁₀H₁₉NO₃
Molecular Weight:201.266
Hs Code.:
Mol file:88155-16-2.mol

Synonyms:Acetamide,N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-,[2R-(2alpha,3alpha,6bta)]-(9CI);Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI)

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Chemical Property of Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI)

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Technology Process of Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI)

There total 5 articles about Acetamide, N-(6-ethoxytetrahydro-2-methyl-2H-pyran-3-yl)-, [2R-(2alpha,3alpha,6ba)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81303-38-0
Ethyl-4,6-di-O-tosyl-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

: 88155-16-2
Ethyl 4-Acetamido-2,3,4,6-tetradeoxy-α-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium azide / dimethylformamide / 12 h / Ambient temperature

2: 1.) H₂; 2.) pyridine / 1.) (10percent) Pd/C / 1.) EtOH, 6 h

With pyridine; sodium azide; hydrogen; 10% palladium on active carbon; In N,N-dimethyl-formamide;

Reference yield:

: 23339-15-3
ethyl 2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 88155-16-2
Ethyl 4-Acetamido-2,3,4,6-tetradeoxy-α-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; CH₂Cl₂ / -30 °C

2: sodium azide / dimethylsulfoxide / 4 h / 140 °C

3: 1.) H₂, 2.) pyridine / 10percent Pd-C / 1.) ethanol, room temperature, 1 atm, 6 h

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In pyridine; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 108-24-7
acetic anhydride

: 81303-42-6
Ethyl-4-azido-2,3,4-tridesoxy-6-O-tosyl-α-D-threo-hex-2-enopyranosid

: 88155-16-2
Ethyl 4-Acetamido-2,3,4,6-tetradeoxy-α-D-threo-hexopyranoside

Guidance literature:: With pyridine; hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) ethanol, room temperature, 1 atm, 6 h;