C₂₉H₃₃BrN₂O₂

Base Information

Chemical Name:C₂₉H₃₃BrN₂O₂
CAS No.:1447766-81-5
Molecular Formula:C₂₉H₃₃BrN₂O₂
Molecular Weight:521.497
Hs Code.:

C<sub>29</sub>H<sub>33</sub>BrN<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₉H₃₃BrN₂O₂

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Chemical Property of C₂₉H₃₃BrN₂O₂

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Technology Process of C₂₉H₃₃BrN₂O₂

There total 6 articles about C₂₉H₃₃BrN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1447766-92-8
C₂₉H₃₅BrN₂O₃

: 1447766-81-5
C₂₉H₃₃BrN₂O₂

Guidance literature:: C₂₉H₃₅BrN₂O₃; With methanesulfonyl chloride; triethylamine; In dichloromethane; for 1.33333h; Inert atmosphere;

With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ja405548b

Reference yield:

: 1447766-83-7
C₂₂H₂₀BrNO₂

: 1447766-81-5
C₂₉H₃₃BrN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: L-proline / dichloromethane; acetonitrile / 216 h / Inert atmosphere

2.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

2.2: 30 h / 20 °C / Inert atmosphere

3.1: sodium iodide; chloro-trimethyl-silane / tetrahydrofuran; acetonitrile / 2 h / Inert atmosphere

4.1: acetic acid; zinc / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere

5.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1.33 h / Inert atmosphere

5.2: 15 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; sodium hydride; acetic acid; methanesulfonyl chloride; triethylamine; L-proline; sodium iodide; zinc; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ja405548b

Reference yield:

: C₂₂H₂₂BrNO₂

: 1447766-81-5
C₂₉H₃₃BrN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: 2.5 h / -78 - 20 °C / Inert atmosphere

2.1: L-proline / dichloromethane; acetonitrile / 216 h / Inert atmosphere

3.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

3.2: 30 h / 20 °C / Inert atmosphere

4.1: sodium iodide; chloro-trimethyl-silane / tetrahydrofuran; acetonitrile / 2 h / Inert atmosphere

5.1: acetic acid; zinc / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere

6.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1.33 h / Inert atmosphere

6.2: 15 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; oxalyl dichloride; sodium hydride; acetic acid; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; L-proline; sodium iodide; zinc; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil; 1.1: |Swern Oxidation;
DOI:10.1021/ja405548b