2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

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Chemical Name:2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate
CAS No.:956427-84-2
Molecular Formula:C₂₆H₂₇N₃O₇S
Molecular Weight:525.582
Hs Code.:

Synonyms:2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

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Chemical Property of 2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

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Technology Process of 2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

There total 5 articles about 2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956427-82-0
di-tert-butyl 2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

: 956427-84-2
2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

Guidance literature:: di-tert-butyl 2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate; With lithium hydroxide; In tetrahydrofuran; methanol; water-d2; at 20 ℃;

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.25h;

Reference yield:

: 956427-80-8
tert-butyl (2-(4-nitrobenzamido)-4-(thiophen-2-yl)phenyl)carbamate

: 956427-84-2
2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethyl acetate

2.1: potassium carbonate; sodium iodide / acetonitrile / 12 h / Heating / reflux

3.1: lithium hydroxide / tetrahydrofuran; methanol; water-d2 / 20 °C

3.2: 0.25 h / 20 °C

With lithium hydroxide; hydrogen; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water-d2; ethyl acetate; acetonitrile;

Reference yield:

: 335255-43-1
tert-butyl 2-amino-4-(thiophen-2-yl)phenylcarbamate

: 956427-84-2
2,2'-{[4-({[2-[(tert-butoxycarbonyl)amino]-5-(2-thienyl)phenyl]amino}carbonyl)phenyl]imino}diacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 1 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethyl acetate

3.1: potassium carbonate; sodium iodide / acetonitrile / 12 h / Heating / reflux

4.1: lithium hydroxide / tetrahydrofuran; methanol; water-d2 / 20 °C

4.2: 0.25 h / 20 °C

With lithium hydroxide; hydrogen; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; water-d2; ethyl acetate; acetonitrile;