3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

Base Information

Chemical Name:3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde
CAS No.:1035216-88-6
Molecular Formula:C₁₈H₁₄Cl₂N₂O₃
Molecular Weight:377.227
Hs Code.:

Synonyms:3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

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Chemical Property of 3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

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Technology Process of 3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

There total 2 articles about 3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1035215-68-9
3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzonitrile

: 1035216-88-6
3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

Guidance literature:: 3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzonitrile; With diisobutylaluminium hydride; In dichloromethane; at -40 ℃; for 2h;

With methanol; In dichloromethane; at -40 - 20 ℃;

Reference yield:

: 181074-22-6
2-chloro-4-cyanobenzoyl chloride

: 1035216-88-6
3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 16 h / 100 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 2 h / -40 °C / Inert atmosphere

2.2: -40 °C / Inert atmosphere

With pyridine; diisobutylaluminium hydride; In dichloromethane;

Reference yield:

: 1035216-88-6
3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde

: 1035217-25-4
ethyl 3-methylazetidine-3-carboxylate

: 1035216-92-2
1-(3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)-3-methylazetidine-3-carboxylic acid ethyl ester

Guidance literature:: 3-chloro-4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzaldehyde; ethyl 3-methylazetidine-3-carboxylate; With acetic acid; In methanol; at 20 ℃; for 1h;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 17h;