4-tert.-butylcyclohexyl methyl ketone

Base Information

• Chemical Name: 4-tert.-butylcyclohexyl methyl ketone
• CAS No.: 19091-09-9
• Molecular Formula: C₁₂H₂₂O
• Molecular Weight: 182.306

Synonyms:4-tert.-butylcyclohexyl methyl ketone

Chemical Property of 4-tert.-butylcyclohexyl methyl ketone

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of 4-tert.-butylcyclohexyl methyl ketone

There total 4 articles about 4-tert.-butylcyclohexyl methyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-t-butylacetophenone (943-27-1) → 4-tert.-butylcyclohexyl methyl ketone (19091-09-9) + 1-(4-tert-butyl-1-cyclohexenyl)ethanol (63767-87-3,61065-77-8)

Guidance literature:

With hydrogen; rhodium; platinum; In acetic acid; for 4h; under 36775.4 Torr; Yield given;

DOI:10.1248/cpb.35.3276

Reference yield:

4'-t-butylacetophenone (943-27-1) → 4-tert.-butylcyclohexyl methyl ketone (19091-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / rhodium-platinium / acetic acid / 4 h / 36775.4 Torr

2: CrO₃, conc. H₂SO₄ / H₂O; acetone / 5 h / Ambient temperature

With chromium(VI) oxide; sulfuric acid; hydrogen; rhodium; platinum; In water; acetic acid; acetone;

DOI:10.1248/cpb.35.3276

Reference yield:

1-(4-tert-butyl-1-cyclohexenyl)ethanol (63767-87-3,61065-77-8) → 4-tert.-butylcyclohexyl methyl ketone (19091-09-9)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water; acetone; for 5h; Ambient temperature;

DOI:10.1248/cpb.35.3276

upstream raw materials:

4'-t-butylacetophenone

1-(4-tert-butyl-1-cyclohexenyl)ethanol

Downstream raw materials:

trans-1-(4'-t-butylcyclohexyl)-1-ethanone

Benzenesulfonic acid 2-(4-tert-butyl-cyclohexyl)-2-oxo-ethyl ester

1-(4-tert-Butyl-cyclohexyl)-2-hydroxy-ethanone

2-Bromo-1-(4-tert-butyl-cyclohexyl)-ethanone

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