N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Base Information

Chemical Name:N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine
CAS No.:82783-15-1
Molecular Formula:C₂₆H₃₇NO₄
Molecular Weight:427.584
Hs Code.:

Synonyms:N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

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Chemical Property of N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

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Technology Process of N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

There total 5 articles about N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.8%

: 69788-93-8
N-ethyl-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

: 82763-37-9
4-<(3,4-dimethoxybenzyl)oxy>butyl bromide

: 82783-15-1
N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Guidance literature:: With sodium iodide; sodium sulfite; In butanone; for 41h; Heating;
DOI:10.1021/jm00353a016

Reference yield:

: 2472-22-2
6-methoxy-2-tetralone

: 82783-15-1
N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol

2: 16.8 percent / NaI, Na₂SO₃ / butan-2-one / 41 h / Heating

With hydrogen; sodium iodide; sodium sulfite; platinum(IV) oxide; In ethanol; butanone;
DOI:10.1021/jm00353a016

Reference yield:

: 82763-35-7
4-<(3,4-dimethoxybenzyl)oxy>-1-butanol

: 82783-15-1
N-ethyl-N-<(3,4-dimethoxybenzyl)oxybutyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / tetrahydrofuran / 24 h / Ambient temperature

2: 75.1 percent / LiBr*H₂O / dimethylformamide / 2 h / 60 °C

3: 16.8 percent / NaI, Na₂SO₃ / butan-2-one / 41 h / Heating

With triethylamine; sodium iodide; lithium bromide; sodium sulfite; In tetrahydrofuran; N,N-dimethyl-formamide; butanone;
DOI:10.1021/jm00353a016