2-Tert-butyl-3-(3-chlorophenyl)oxaziridine

Base Information

Chemical Name:2-Tert-butyl-3-(3-chlorophenyl)oxaziridine
CAS No.:23898-59-1
Molecular Formula:C₁₁H₁₄ClNO
Molecular Weight:211.691
Hs Code.:
NSC Number:116593
DSSTox Substance ID:DTXSID00297554
Mol file:23898-59-1.mol

Synonyms:23898-59-1;2-tert-butyl-3-(3-chlorophenyl)oxaziridine;NSC116593;DTXSID00297554;NSC-116593

Suppliers and Price of 2-Tert-butyl-3-(3-chlorophenyl)oxaziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Tert-butyl-3-(3-chlorophenyl)oxaziridine

Chemical Property:

Vapor Pressure:0.0171mmHg at 25°C
Boiling Point:254.6°C at 760 mmHg
Flash Point:107.8°C
Density:1.191g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:211.0763918
Heavy Atom Count:14
Complexity:214

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)N1C(O1)C2=CC(=CC=C2)Cl

Technology Process of 2-Tert-butyl-3-(3-chlorophenyl)oxaziridine

There total 2 articles about 2-Tert-butyl-3-(3-chlorophenyl)oxaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 116451-07-1
tert-Butyl-[1-(3-chloro-phenyl)-meth-(E)-ylidene]-amine

: 23898-59-1,116450-95-4
(2R,3R)-2-tert-Butyl-3-(3-chloro-phenyl)-oxaziridine

Guidance literature:: With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; 1.) -15 deg C, 1.5 h, 2.) -15 deg C to 0 deg C, 3 h;
DOI:10.1055/s-1987-28176

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 23898-59-1,116450-95-4
(2R,3R)-2-tert-Butyl-3-(3-chloro-phenyl)-oxaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / molecular sieves (Serva 4a) / 24 h / Ambient temperature

2: 60 percent / m-chloroperoxybenzoic acid, Na₂CO₃ / CHCl₃ / 1.) -15 deg C, 1.5 h, 2.) -15 deg C to 0 deg C, 3 h

With 4 A molecular sieve; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1055/s-1987-28176