2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

Base Information

Chemical Name:2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl
CAS No.:206991-10-8
Molecular Formula:C₁₃H₁₆N₅O₂
Molecular Weight:274.302
Hs Code.:

Synonyms:2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

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Chemical Property of 2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

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Technology Process of 2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

There total 4 articles about 2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 364038-65-3
2-(4-azidophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

: 206991-10-8
2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

Guidance literature:: With sodium periodate; In chloroform; water; at 20 ℃; for 0.0833333h;
DOI:10.1021/jo049500r

Reference yield:

: 24173-36-2
4-azidobenzaldehyde

: 14538-51-3,78375-92-5
2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate

: 206991-10-8
2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

Guidance literature:: With sodium periodate; Multistep reaction; 2.) CHCl₃;
DOI:10.1021/ja980120v

Reference yield:

: 24173-36-2
4-azidobenzaldehyde

: 206991-10-8
2-(4-azidophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-3-oxide-1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / methanol / 24 h / 20 °C

2: NaIO₄ / CHCl₃; H₂O / 0.08 h / 20 °C

With sodium periodate; triethylamine; In methanol; chloroform; water;
DOI:10.1021/jo049500r