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Technology Process of pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)

pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)

Base Information
  • Chemical Name:pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)
  • CAS No.:864685-88-1
  • Molecular Formula:C24H37Cl2NOTi
  • Molecular Weight:474.35
  • Hs Code.:
pentamethylcyclopentadienyl titanium dichloride (OCH<sub>2</sub>CH<sub>2</sub>NHC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)

Synonyms:pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)

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Chemical Property of pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)
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Technology Process of pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)

There total 1 articles about pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Cp*TiCl<sub>3</sub>
12129-06-5

Cp*TiCl3

2-(2,6-diisopropylphenylamino)ethanol

2-(2,6-diisopropylphenylamino)ethanol

pentamethylcyclopentadienyl titanium dichloride (OCH<sub>2</sub>CH<sub>2</sub>NHC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)
864685-88-1

pentamethylcyclopentadienyl titanium dichloride (OCH2CH2NHC6H3(CH(CH3)2)2)

Guidance literature:
With Et3N; In dichloromethane; ligand and Et3N in CH2Cl2 treated dropwise with Ti complexes in CH2Cl2 under stirring at -78°C, warmed to room temp., stirred for 12 h; evapd.(vac.), redissolved (toluene), filtered (celite), evapd., elem. anal.;
DOI:10.1016/j.molcata.2005.01.007
upstream raw materials:

Cp*TiCl3

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