Technology Process of [5-(4-(1-methylpyridinium))-10,15,20-triphenyl-porphyrinato]manganese(III) dichloride
There total 1 articles about [5-(4-(1-methylpyridinium))-10,15,20-triphenyl-porphyrinato]manganese(III) dichloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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With
air;
In
N,N-dimethyl-formamide;
porphyrine and excess MnCl2*4H2O dissolved in degassed DMF; stirred in inert atmosphere (80°C overnight); left in open air (30 min); solvent removed (vac.); solid dissolved in CHCl3; filtered; washed with 5% aq. HCl and then with brine until neutrality; org. phase dried (Na2SO4); solvent removed (vac.) recrystd. from CH2Cl2/hexne;
DOI:10.1016/S1381-1169(01)00406-X