C₂₂H₃₄O₇

Base Information

Chemical Name:C₂₂H₃₄O₇
CAS No.:1286242-16-7
Molecular Formula:C₂₂H₃₄O₇
Molecular Weight:410.508
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>7</sub>

Synonyms:C₂₂H₃₄O₇

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Chemical Property of C₂₂H₃₄O₇

Chemical Property:

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Technology Process of C₂₂H₃₄O₇

There total 18 articles about C₂₂H₃₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1286242-13-4
C₃₈H₅₂O₇Si

: 1286242-16-7
C₂₂H₃₄O₇

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-94-8
C₃₁H₄₈O₄Si₂

: 1286242-16-7
C₂₂H₃₄O₇

Guidance literature:: Multi-step reaction with 14 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

3: Dess-Martin periodane / dichloromethane

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

5: trimethylaluminum / dichloromethane; water / -50 °C

6: toluene-4-sulfonic acid / benzene / Reflux

7: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

8: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

9: copper(l) cyanide / diethyl ether / -50 - -30 °C

10: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

11: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

12: diethyl ether / 0 °C

13: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / Reflux

14: tetrabutyl ammonium fluoride; acetic acid / N,N-dimethyl-formamide

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene; 2: Katsuki-Sharpless epoxidation / 3: Dess-Martin oxidation / 3: Wittig reaction / 8: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-97-1
C₃₀H₄₈O₄Si₂

: 1286242-16-7
C₂₂H₃₄O₇

Guidance literature:: Multi-step reaction with 12 steps

1: Dess-Martin periodane / dichloromethane

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

3: trimethylaluminum / dichloromethane; water / -50 °C

4: toluene-4-sulfonic acid / benzene / Reflux

5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

6: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

7: copper(l) cyanide / diethyl ether / -50 - -30 °C

8: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

9: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

10: diethyl ether / 0 °C

11: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / Reflux

12: tetrabutyl ammonium fluoride; acetic acid / N,N-dimethyl-formamide

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene; 1: Dess-Martin oxidation / 1: Wittig reaction / 6: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106