(1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

Base Information

Chemical Name:(1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide
CAS No.:613241-84-2
Molecular Formula:C₁₀H₁₈O₄
Molecular Weight:202.251
Hs Code.:

Synonyms:(1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

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Chemical Property of (1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

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Technology Process of (1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

There total 4 articles about (1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 5989-54-8,555-08-8,8022-90-0,9003-73-0,95327-98-3
(-)-(S)-limonene

: 613241-83-1
1-methyl-1-(4-methyl-3-cyclohexenyl)ethyl hydroperoxide

: 613241-84-2
(1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

Guidance literature:: (-)-(S)-limonene; With triethylsilane; bis(1-morpholinocarbamoyl-4,4-dimethyl-1,3-pentanedionato)Co; oxygen; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

With hydrogenchloride; In methanol; water; for 0.0833333h;
DOI:10.1021/jo030107f

Reference yield: 23.0%

: 5989-54-8,555-08-8,8022-90-0,9003-73-0,95327-98-3
(-)-(S)-limonene

: 613241-83-1
1-methyl-1-(4-methyl-3-cyclohexenyl)ethyl hydroperoxide

: 4-(1-hydroperoxy-1-methylethyl)-1-methylcyclohexyl hydroperoxide

: 613241-84-2
(1S,5S,8S)-4,4,8-trimethyl-2,3-dioxabicyclo[3.3.1]nonan-8-yl hydroperoxide

Guidance literature:: (-)-(S)-limonene; With triethylsilane; bis(1-morpholinocarbamoyl-4,4-dimethyl-1,3-pentanedionato)Co; oxygen; In 1,2-dichloro-ethane; at 20 ℃; for 24h;

With hydrogenchloride; In methanol; water; for 0.0833333h;
DOI:10.1021/jo030107f