(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

Base Information

Chemical Name:(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam
CAS No.:155203-58-0
Molecular Formula:C₂₄H₃₂N₂O₄S
Molecular Weight:444.595
Hs Code.:

Synonyms:(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

Suppliers and Price of (2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

There total 1 articles about (2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 155203-59-1
(2S,2'S)-N-(2',3',4',5'-tetrahydro-1'-oxido-1'-pyridinio-2'-carbonyl)bornane-10,2-sultam

: 108448-77-7,124224-04-0
(+)-camphorsultam

: (2S,2'S,3'aR,7'R)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

: 155203-58-0
(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

Guidance literature:: In dichloromethane; for 2h; Yield given. Yields of byproduct given; Heating;
DOI:10.1002/hlca.19940770217

Reference yield: 91.0%

: 155203-58-0
(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

: 108448-77-7,124224-04-0
(+)-camphorsultam

: 155203-62-6
(2R,3aS,7S)-3,3a,4,5,6,7-hexahydro-2-phenyl-2H-isoxazolo<2,3-a>pyridine-7-carboxylic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 55 ℃; for 30h;
DOI:10.1002/hlca.19940770217

Reference yield:

: 155203-58-0
(2R,2'R,3'aS,7'S)-N-(3',3'a,4',5',6',7'-hexahydro-2'-phenyl-2'H-isooxazolo<2,3a>-pyridine-7'-carbonyl)bornane-10,2-sultam

: 155203-63-7
(2R,3aS,7S)-3,3a,4,5,6,7-hexahydro-2-phenyl-2H-isoxazolo<2,3-a>pyridine-7-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 30 h / 55 °C

2: N-methylmorpholine / tetrahydrofuran / 0.17 h / -15 °C

3: NH₃ / tetrahydrofuran / -15 deg C, 30 min, and room t.

With 4-methyl-morpholine; lithium hydroxide; ammonia; In tetrahydrofuran; water;
DOI:10.1002/hlca.19940770217