dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate

Base Information

• Chemical Name: dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate
• CAS No.: 1207373-42-9
• Molecular Formula: C₃₀H₂₉N₂O₆PS
• Molecular Weight: 576.61

Synonyms:dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate

Chemical Property of dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate

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Technology Process of dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate

There total 1 articles about dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl 2-{[(2-azidophenyl)sulfonyl]amino}succinate (1207374-15-9) + triphenylphosphine (603-35-0) → dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate (1207373-42-9)

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

Reference yield: 98.0%

dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate (1207373-42-9) + phenyl isocyanate (103-71-9) → methyl (5,5-dioxido-2-oxo-1-phenyl-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl)acetate (1207373-65-6)

Guidance literature:

In toluene; at 110 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

Reference yield: 88.0%

dimethyl 2-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]succinate (1207373-42-9) + p-Tolylisocyanate (622-58-2,374675-64-6) → methyl [1-(4-methylphenyl)-5,5-dioxido-2-oxo-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl]acetate (1207373-66-7)

Guidance literature:

In toluene; at 110 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

upstream raw materials:

dimethyl 2-{[(2-azidophenyl)sulfonyl]amino}succinate

triphenylphosphine

Downstream raw materials:

methyl [1-(4-chlorophenyl)-5,5-dioxido-2-oxo-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl]acetate

methyl (5,5-dioxido-2-oxo-1-phenyl-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl)acetate

methyl [1-(4-methylphenyl)-5,5-dioxido-2-oxo-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl]acetate

methyl [1-(4-methoxyphenyl)-5,5-dioxido-2-oxo-2,3-dihydro-1H-imidazo[1,2-b][1,2,4]benzothiadiazin-3-yl]acetate

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