C₃₄H₃₉N₅O₅S

Base Information

Chemical Name:C₃₄H₃₉N₅O₅S
CAS No.:1373961-50-2
Molecular Formula:C₃₄H₃₉N₅O₅S
Molecular Weight:629.78
Hs Code.:

C<sub>34</sub>H<sub>39</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:C₃₄H₃₉N₅O₅S

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Chemical Property of C₃₄H₃₉N₅O₅S

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Technology Process of C₃₄H₃₉N₅O₅S

There total 8 articles about C₃₄H₃₉N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1373961-49-9
C₂₆H₂₉N₃O₆

: 1373961-50-2
C₃₄H₃₉N₅O₅S

Guidance literature:: C₂₆H₂₉N₃O₆; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 21368-39-8
dimethyl 5-(prop-2-en-1-yloxy)benzene-1,3-dicarboxylate

: 1373961-50-2
C₃₄H₃₉N₅O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,N-diethylaniline / 24 h / 195 °C / Inert atmosphere

2.1: copper diacetate; oxygen / acetonitrile / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Inert atmosphere

4.1: hydrogen / palladium 10% on activated carbon / methanol

5.1: sodium hydroxide; methanol / tetrahydrofuran / 4 h / 0 °C

5.2: pH 2

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C

7.1: Burgess Reagent / 1,2-dichloro-ethane / Inert atmosphere; Reflux

8.1: sodium hydroxide; methanol / tetrahydrofuran

8.2: pH 2

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

9.2: 0 - 20 °C

With methanol; Burgess Reagent; hydrogen; oxygen; copper diacetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N,N-diethylaniline; sodium hydroxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 1373961-50-2
C₃₄H₃₉N₅O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C / Inert atmosphere

2.1: N,N-diethylaniline / 24 h / 195 °C / Inert atmosphere

3.1: copper diacetate; oxygen / acetonitrile / Inert atmosphere

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / methanol

6.1: sodium hydroxide; methanol / tetrahydrofuran / 4 h / 0 °C

6.2: pH 2

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.2: 0 - 20 °C

8.1: Burgess Reagent / 1,2-dichloro-ethane / Inert atmosphere; Reflux

9.1: sodium hydroxide; methanol / tetrahydrofuran

9.2: pH 2

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

10.2: 0 - 20 °C

With methanol; Burgess Reagent; hydrogen; oxygen; copper diacetate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N,N-diethylaniline; sodium hydroxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;