Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

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Chemical Name:Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester
CAS No.:78515-23-8
Molecular Formula:C₂₆H₂₈O₁₀
Molecular Weight:500.502
Hs Code.:

Synonyms:Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

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Chemical Property of Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

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Technology Process of Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

There total 2 articles about Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 78515-17-0
Succinic acid 5-formyl-2-methoxy-phenyl ester methyl ester

: 78515-23-8
Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

Guidance literature:: With titanium(III) chloride; copper; zinc; In 1,2-dimethoxyethane; for 16h; Heating;
DOI:10.1021/jo00334a039

Reference yield:

: 621-59-0
isovanillin

: 78515-23-8
Succinic acid 2-methoxy-5-{(E)-2-[4-methoxy-3-(3-methoxycarbonyl-propionyloxy)-phenyl]-vinyl}-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 4-(dimethylamino)pyridine / 1.) pyridine, r.t., 2 d, 2.) ether, ice bath, 20 min

2: 60 percent / TiCl₃, Zn-Cu couple / 1,2-dimethoxy-ethane / 16 h / Heating

With dmap; titanium(III) chloride; copper; zinc; In 1,2-dimethoxyethane;
DOI:10.1021/jo00334a039