C₄₃H₆₈O₇Si₂

Base Information

Chemical Name:C₄₃H₆₈O₇Si₂
CAS No.:1225339-88-7
Molecular Formula:C₄₃H₆₈O₇Si₂
Molecular Weight:753.18
Hs Code.:

C<sub>43</sub>H<sub>68</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₄₃H₆₈O₇Si₂

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Chemical Property of C₄₃H₆₈O₇Si₂

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Technology Process of C₄₃H₆₈O₇Si₂

There total 1 articles about C₄₃H₆₈O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1225339-83-2
C₂₇H₂₇O₇P

: 1225339-82-1
C₂₈H₅₀O₄Si₂

: 1225339-88-7
C₄₃H₆₈O₇Si₂

Guidance literature:: C₂₈H₅₀O₄Si₂; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 ℃;

C₂₇H₂₇O₇P; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 50 ℃; for 1h;
DOI:10.1021/ol102925d

Reference yield: 77.0%

: 1225339-88-7
C₄₃H₆₈O₇Si₂

: 1225339-89-8
C₄₃H₇₀O₈Si₂

Guidance literature:: C₄₃H₆₈O₇Si₂; With dimethylsulfide borane complex; at 0 - 20 ℃;

With dihydrogen peroxide; sodium hydroxide; In water; at 0 - 20 ℃; stereoselective reaction;
DOI:10.3987/COM-09-S(S)93

Reference yield:

: 1225339-88-7
C₄₃H₆₈O₇Si₂

: 1264660-90-3
C₆₀H₇₈O₁₁

Guidance literature:: Multi-step reaction with 14 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

2.2: 2.5 h

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

5.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

6.2: 15 h

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

8.1: n-heptane; dichloromethane / -78 - 0 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

10.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

11.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

12.1: diethyl ether / -78 - 0 °C

13.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C

13.2: 0.33 h / -78 °C

14.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; triethylsilane; n-butyllithium; tetrapropylammonium perruthennate; trimethylsilyl trifluoromethanesulfonate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 13.2: Aldol condensation;
DOI:10.1021/ol102925d