C₃₇H₃₈ClN₅O₆

Base Information

Chemical Name:C₃₇H₃₈ClN₅O₆
CAS No.:1369595-51-6
Molecular Formula:C₃₇H₃₈ClN₅O₆
Molecular Weight:684.192
Hs Code.:

C<sub>37</sub>H<sub>38</sub>ClN<sub>5</sub>O<sub>6</sub>

Synonyms:C₃₇H₃₈ClN₅O₆

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Chemical Property of C₃₇H₃₈ClN₅O₆

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Technology Process of C₃₇H₃₈ClN₅O₆

There total 15 articles about C₃₇H₃₈ClN₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: C₃₀H₂₇ClN₄O₃*2ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1369595-51-6
C₃₇H₃₈ClN₅O₆

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-51-6
C₃₇H₃₈ClN₅O₆

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / ethanol / 15 h / 90 °C

2: polyphosphoric acid / 2 h / 110 °C

3: caesium carbonate / dimethyl sulfoxide / 21 h / 100 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 2 h / 90 °C

5: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 3 h / 90 °C

6: hydrogenchloride / 1,4-dioxane; methanol / 18 h / 20 °C

7: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 °C

With hydrogenchloride; potassium acetate; potassium carbonate; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1369595-51-6
C₃₇H₃₈ClN₅O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonia / methanol / 0.5 h / 20 - 30 °C

1.2: 16 h / 20 - 60 °C

2.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

3.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 3 h / 90 °C

4.1: hydrogenchloride / 1,4-dioxane; methanol / 18 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 °C

With hydrogenchloride; N-Bromosuccinimide; ammonia; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;