di[(R)-2-ethylhexyl] phthalate

Base Information

Chemical Name:di[(R)-2-ethylhexyl] phthalate
CAS No.:74746-55-7
Molecular Formula:C₂₄H₃₈O₄
Molecular Weight:390.563
Hs Code.:

Synonyms:di[(R)-2-ethylhexyl] phthalate

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Chemical Property of di[(R)-2-ethylhexyl] phthalate

Chemical Property:

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Technology Process of di[(R)-2-ethylhexyl] phthalate

There total 6 articles about di[(R)-2-ethylhexyl] phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 85-44-9
phthalic anhydride

: 50373-29-0
(R)-2-ethylhexanol

: 74746-55-7,275818-89-8,50885-87-5,82208-43-3,607374-50-5,8033-53-2
di[(R)-2-ethylhexyl] phthalate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 4h; Dean-Stark; Reflux;
DOI:10.2174/1570178616666190718125617

Reference yield:

: trans-2-ethyl-2-hexenoyl chloride

: 74746-55-7,275818-89-8,50885-87-5,82208-43-3,607374-50-5,8033-53-2
di[(R)-2-ethylhexyl] phthalate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C

1.2: 18 h / 20 °C

2.1: hydrogen; palladium on activated charcoal / ethanol / 16 h / 25 °C

3.1: sodium tetrahydroborate; water / tetrahydrofuran / 16 h / 0 - 25 °C

4.1: toluene-4-sulfonic acid / toluene / 4 h / Dean-Stark; Reflux

With sodium tetrahydroborate; n-butyllithium; palladium on activated charcoal; water; hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; hexane; toluene;
DOI:10.2174/1570178616666190718125617

Reference yield:

: 64344-45-2
(E)-2-ethyl-2-hexenal

: 74746-55-7,275818-89-8,50885-87-5,82208-43-3,607374-50-5,8033-53-2
di[(R)-2-ethylhexyl] phthalate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 12 h / 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 4.5 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C

3.2: 18 h / 20 °C

4.1: hydrogen; palladium on activated charcoal / ethanol / 16 h / 25 °C

5.1: sodium tetrahydroborate; water / tetrahydrofuran / 16 h / 0 - 25 °C

6.1: toluene-4-sulfonic acid / toluene / 4 h / Dean-Stark; Reflux

With sodium chlorite; sodium tetrahydroborate; potassium dihydrogenphosphate; n-butyllithium; oxalyl dichloride; palladium on activated charcoal; water; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.2174/1570178616666190718125617