hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride

Base Information

• Chemical Name: hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride
• CAS No.: 95123-22-1
• Molecular Formula: C₄₃H₄₀O₂P₃Ru*Cl
• Molecular Weight: 818.234

Synonyms:hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride

Chemical Property of hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride

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Technology Process of hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride

There total 5 articles about hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽¹⁺⁾ chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Ru(CO)2(CH3C(CH2P(C6H5)2)3) (37843-33-7) → hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(1+) chloride (95123-22-1)

Guidance literature:

With Me₂CHC(O)Cl; In dichloromethane; byproducts: Me2C=C=O; N2 atmosphere; refluxing (2-3 d), IR control;

DOI:10.1016/0022-328X(88)80510-2

Reference yield:

Ru(CO)2(CH3C(CH2P(C6H5)2)3) (37843-33-7) → Ketene (463-51-4) + hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(1+) chloride (95123-22-1)

Guidance literature:

With acetyl chloride; In dichloromethane; React. of equimolar amt. of Ru-compd. with MeCOCl in CH2Cl2 (room temp.) is monitored by FTIR.;

DOI:10.1021/ja00294a056

Reference yield:

dicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(0) (37843-33-7) → Ketene (463-51-4) + hydridodicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium(1+) chloride (95123-22-1)

Guidance literature:

With acetyl chloride; In dichloromethane; under N2, equimolar amts. of Ru(CO)2(triphos) and MeCOCl allowed to react in CH2Cl2 at room temp. up to 20 h; not isolated; monitored by IR; Kinetics;

upstream raw materials:

Ru(CO)2(CH₃C(CH₂P(C₆H₅)2)3)

dicarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium⁽⁰⁾

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