3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

Base Information

Chemical Name:3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol
CAS No.:102275-64-9
Molecular Formula:C₂₅H₂₉NO₄S
Molecular Weight:439.576
Hs Code.:

Synonyms:3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

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Chemical Property of 3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

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Technology Process of 3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

There total 5 articles about 3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 102275-63-8
3,6-Bis-(3,3-dimethylallyl)-1-tosylindol

: 102275-64-9
3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; 1.) -10 deg C, 1 h, 2.) room temp., 3 h;
DOI:10.1002/ardp.19853181219

Reference yield:

: 73618-54-9
3,6-Bis-(3,3-dimethylallyl)-indol

: 102275-64-9
3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 1.) NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

2: 58 percent / 3-chloroperoxybenzoic acid / CHCl₃ / 1.) -10 deg C, 1 h, 2.) room temp., 3 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/ardp.19853181219

Reference yield:

: 23158-16-9
6-(3-methylbut-2-en-1-yl)-1H-indole

: 102275-64-9
3,6-Di-(2,3-epoxy-3-methylbutyl)-1-tosylindol

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / sodium acetate / aq. acetic acid / 1 h

2: 79 percent / 1.) NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

3: 58 percent / 3-chloroperoxybenzoic acid / CHCl₃ / 1.) -10 deg C, 1 h, 2.) room temp., 3 h

With sodium acetate; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/ardp.19853181219