Technology Process of C46H44N4O14
There total 3 articles about C46H44N4O14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran;
at 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1016/j.tet.2012.01.080
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; ethyl acetate / 10 h / 20 °C / Inert atmosphere
2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.tet.2012.01.080
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / dichloromethane / 21 h / Inert atmosphere; Reflux
2: hydrogenchloride / water; ethyl acetate / 10 h / 20 °C / Inert atmosphere
3: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; hydrogenchloride; 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.tet.2012.01.080
