methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

Base Information

Chemical Name:methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt
CAS No.:1071521-05-5
Molecular Formula:C₈H₈O₃*C₁₅H₁₈FNO₃
Molecular Weight:431.461
Hs Code.:

Synonyms:methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

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Chemical Property of methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

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Technology Process of methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

There total 2 articles about methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 17199-29-0
(S)-Mandelic acid

: (rac-di-exo)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylic acid methyl ester

: 1071521-05-5
methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

Guidance literature:: In ethyl acetate;

Reference yield:

: 665054-35-3
(rac-di-exo)-3-amino-7-oxabicyclo[2.2.1]heptane-2-carboxylic acid

: 1071521-05-5
methyl (1R,2S,3R,4S)-3-(4-fluorobenzylamino)-7-oxabicyclo[2.2.1]heptane-2-carboxylate mandelic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / benzene; diethyl ether

2.1: methanol / 0.17 h / 25 °C / Inert atmosphere

2.2: 18 h / 25 °C

3.1: ethyl acetate

With methanol; In methanol; diethyl ether; ethyl acetate; benzene;