benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

Base Information

Chemical Name:benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate
CAS No.:925685-12-7
Molecular Formula:C₂₉H₄₂O₉P₂
Molecular Weight:596.595
Hs Code.:

Synonyms:benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

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Chemical Property of benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

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Technology Process of benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

There total 7 articles about benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 925685-08-1
benzyl 3-(2-hydroxy-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

: 79-30-1
isobutyryl chloride

: 925685-12-7
benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

Guidance literature:: With pyridine; dmap; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm801007z

Reference yield:

: 164012-31-1
4,4-dimethyl-6-bromo-2-oxo-chroman

: 925685-12-7
benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 18 h / 100 °C

2.1: potassium hydroxide / methanol / 2 h / 20 °C

2.2: pH 4

3.1: potassium hydroxide / water; acetonitrile / 0.17 h

4.1: potassium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: pyridine / dmap / 2 h / 20 °C

With pyridine; potassium hydroxide; triethylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 925685-06-9
6-(ethoxy(diethylphosphonomethyl)phosphinoyl)-3,4-dihydro-4,4-dimethylchromen-2-one

: 925685-12-7
benzyl 3-(2-(2,2-dimethylacetoxy)-5-(ethoxy(diethylphosphonomethyl)phosphinoyl)phenyl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / methanol / 2 h / 20 °C

1.2: pH 4

2.1: potassium hydroxide / water; acetonitrile / 0.17 h

3.1: potassium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: pyridine / dmap / 2 h / 20 °C

With pyridine; potassium hydroxide; dmap; In methanol; water; N,N-dimethyl-formamide; acetonitrile;