4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

Base Information

Chemical Name:4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride
CAS No.:1606976-40-2
Molecular Formula:C₁₄H₁₁Cl₂N*ClH
Molecular Weight:300.615
Hs Code.:

Synonyms:4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

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Chemical Property of 4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

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Technology Process of 4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

There total 1 articles about 4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1187830-87-0
2,4-dichloro-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloric acid salt

: 63503-60-6
3-chlorophenylboronic acid

: 1606976-40-2
4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

Guidance literature:: 2,4-dichloro-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloric acid salt; 3-chlorophenylboronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 90 ℃; for 4h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane;

Reference yield: 100.0%

: 1606976-40-2
4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

: 91361-92-1
(4-mercapto-phenyl)-acetic acid methyl ester

: methyl 2-(4-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)thio)phenyl)acetate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1021/acs.jmedchem.9b00193

Reference yield: 91.0%

: 1606976-40-2
4-chloro-2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine hydrochloride

: 52913-11-8
(3-amino-phenyl)-acetic acid methyl ester

: 1606973-92-5
methyl 2-(3-((2-(3-chlorophenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)amino)phenyl)acetate hydrochloride

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; Inert atmosphere; Heating;
DOI:10.1021/acs.jmedchem.9b00193