[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Base Information

Chemical Name:[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄
CAS No.:89823-73-4
Molecular Formula:C₄₅H₃₉ClNOP₂RuS*ClO₄
Molecular Weight:939.798
Hs Code.:

[RuCl(H<sub>2</sub>O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO<sub>4</sub>

Synonyms:[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Suppliers and Price of [RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

There total 1 articles about [RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75861-90-4,75880-84-1,89886-99-7
cis-RuCl₂(CS)(p-tolylisocyanide)(triphenylphosphine)2

: silver perchlorate

: 89823-73-4
[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Guidance literature:: In ethanol; dichloromethane; byproducts: AgCl; addn. of AgClO4 in EtOH to Ru-complex in CH2Cl2, stirring (20 min); filtration off of AgCl (celite), CH2Cl2 removal, recrystn. (CH2Cl2/EtOH);
DOI:10.1016/0022-328X(83)89509-6

Reference yield: 97.1%

: 89823-73-4
[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

: 75861-92-6,89887-02-5
[RuCl(CO)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

Guidance literature:: With carbon monoxide; In ethanol; dichloromethane; CH2Cl2/EtOH=3:2 v/v, 500 kPa CO, 100°C, 5 min; cooling, crystn. on volume reduction (reduced pressure); elem. anal.;
DOI:10.1016/0022-328X(83)89509-6

Reference yield: 93.0%

: 89823-73-4
[RuCl(H₂O)(CS)(p-tolylisocyanide)(triphenylphosphine)2]ClO₄

: 7175-47-5
4-methylphenyl isocyanide

: 89823-75-6
[RuCl(CS)(p-tolylisocyanide)2(triphenylphosphine)2]ClO₄

Guidance literature:: In ethanol; dichloromethane; addn. of isocyanide in EtOH to Ru-complex in CH2Cl2, stirring (5 min); addn. of EtOH, CH2Cl2 removal, washing (EtOH, hexane); can be recrystallized (CH2Cl2/EtOH/cyclohexane); elem. anal.;
DOI:10.1016/0022-328X(83)89509-6