Technology Process of C15H22O3S
There total 8 articles about C15H22O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(2S)-2-hydroxy-1((R)-p-tolylsulfinyl)-oct-7-en-4-one;
With
diethyl methoxy borane;
In
tetrahydrofuran; methanol;
at -78 ℃;
for 0.333333h;
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
at -78 ℃;
for 4h;
DOI:10.1039/c2ob26641e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
2.1: 10-camphorsufonic acid / acetone / 24 h / 20 °C
3.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.33 h / -78 °C
3.2: 4 h / -78 °C
With
diethyl methoxy borane; 10-camphorsufonic acid; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; acetone; toluene;
DOI:10.1039/c2ob26641e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 5 h / -78 °C
2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
3.1: 10-camphorsufonic acid / acetone / 24 h / 20 °C
4.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.33 h / -78 °C
4.2: 4 h / -78 °C
With
n-butyllithium; diethyl methoxy borane; 10-camphorsufonic acid; diisobutylaluminium hydride; diisopropylamine;
In
tetrahydrofuran; methanol; hexane; acetone; toluene;
DOI:10.1039/c2ob26641e