[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)

Base Information

• Chemical Name: [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)
• CAS No.: 258519-01-6
• Molecular Formula: C₂₄BF₂₀*C₂₅H₅₅Al₂N₄
• Molecular Weight: 1144.74

Synonyms:[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)

Chemical Property of [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)

There total 1 articles about [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

((t)BuC(N(isopropyl))2)AlMe2 (194655-52-2) + trityl tetrakis(pentafluorophenyl)borate → [((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*B(C6F5)4(1-) (258519-01-6) + Triphenylethan (5271-39-6)

Guidance literature:

In further solvent(s); in sealed tube, soln. in C6D5Cl, 23°C, 15 min; not isolated; NMR;

DOI:10.1021/ja992104j

Reference yield:

[((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*B(C6F5)4(1-) (258519-01-6) → [((CH3)3CC(NCH(CH3)2)2)Al(CH3)(N(CH3)2C6H5)](1+)*[B(C6F5)4](1-)=[((CH3)3CC(NCH(CH3)2)2)Al(CH3)(N(CH3)2C6H5)][B(C6F5)4] (194655-55-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane-d2

2: dichloromethane-d2

In dichloromethane-d2;

DOI:10.1021/ja992104j

Reference yield:

[((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*B(C6F5)4(1-) (258519-01-6) → ((CH3)3CC(NCH(CH3)2)2)Al(CH3)(C6F5) (258519-16-3)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane-d2

2: further solvent(s)

In dichloromethane-d2;

DOI:10.1021/ja992104j

upstream raw materials:

((t)BuC(N(isopropyl))2)AlMe₂

Downstream raw materials:

((t)BuC(N(isopropyl))2)AlMe₂

[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)(N(CH₃)2C₆H₅)]⁽¹⁺⁾*[B(C₆F₅)4]^(1-)=[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)(N(CH₃)2C₆H₅)][B(C₆F₅)4]

((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)(C₆F₅)

[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)

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