Technology Process of C15H12N2O
There total 5 articles about C15H12N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
2: methanol / 20 °C
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; methanol;
2: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.bmcl.2014.03.026
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / dichloromethane / Reflux
2: triethylamine / dichloromethane / 20 °C
3: tris-(dibenzylideneacetone)dipalladium(0); XPhos; potassium carbonate / tert-butyl alcohol / Reflux
4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
5: methanol / 20 °C
With
tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; triethylamine; XPhos;
In
tetrahydrofuran; methanol; dichloromethane; tert-butyl alcohol;
3: |Buchwald-Hartwig Coupling / 5: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.bmcl.2014.03.026