(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

Base Information

Chemical Name:(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate
CAS No.:173168-52-0
Molecular Formula:C₁₅H₂₄ClO₄P
Molecular Weight:334.78
Hs Code.:

Synonyms:(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

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Technology Process of (R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

There total 1 articles about (R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 89-98-5
2-chloro-benzaldehyde

: 13086-84-5
di-tert-butyl phosphite

: 173168-52-0
(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h;

Reference yield: 77.0%

: 173168-52-0
(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

: 173168-59-7
Di-tert-butyl 2-chlorobenzoylphosphonate

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 72h; Ambient temperature;

Reference yield:

: 173168-52-0
(R,S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

: (S)-Di-tert-butyl (2-chlorophenyl)hydroxymethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / PDC / CH₂Cl₂ / 72 h / Ambient temperature

2: catecholborane / (S)-2-butyl-5,5-diphenyl-3,4-trimethylene-1,3,2-oxazaborolidine / toluene / 5 h / -20 °C

With dipyridinium dichromate; benzo[1,3,2]dioxaborole; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In dichloromethane; toluene;