((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane
CAS No.:835594-87-1
Molecular Formula:C₁₉H₃₂OSiTe
Molecular Weight:432.148
Hs Code.:

Synonyms:((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

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Chemical Property of ((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Chemical Property:

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Technology Process of ((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

There total 5 articles about ((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 109-72-8,29786-93-4
n-butyllithium

: 160309-16-0
(R)-(-)-(1-phenyl-prop-2-ynyloxy)(tert-butyl)dimethylsilane

: 835594-87-1
((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Guidance literature:: n-butyllithium; With tellurium; In tetrahydrofuran; hexane; at 20 ℃; for 0.0833333h;

(R)-(-)-(1-phenyl-prop-2-ynyloxy)(tert-butyl)dimethylsilane; In tetrahydrofuran; ethanol; hexane; Heating;
DOI:10.1016/j.tet.2004.10.087

Reference yield:

: 4187-87-5
1-Phenyl-2-propyn-1-ol

: 835594-87-1
((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 46 percent / Novozyme 435 / hexane / 0.67 h / 32 °C

2.1: 95 percent / K₂CO₃ / methanol; H₂O / 12 h / 20 °C

3.1: 80 percent / imidazole / CHCl₃ / 12 h / 20 °C

4.1: tellurium / tetrahydrofuran; hexane / 0.08 h / 20 °C

4.2: 72 percent / tetrahydrofuran; hexane; ethanol / Heating

With 1H-imidazole; tellurium; novozyme 435; potassium carbonate; In tetrahydrofuran; methanol; hexane; chloroform; water;
DOI:10.1016/j.tet.2004.10.087

Reference yield:

: 4187-87-5,64599-56-0,64937-86-6,61317-73-5
(R)-1-phenyl-2-propyn-1-ol

: 835594-87-1
((R,Z)-(-)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / imidazole / CHCl₃ / 12 h / 20 °C

2.1: tellurium / tetrahydrofuran; hexane / 0.08 h / 20 °C

2.2: 72 percent / tetrahydrofuran; hexane; ethanol / Heating

With 1H-imidazole; tellurium; In tetrahydrofuran; hexane; chloroform;
DOI:10.1016/j.tet.2004.10.087