6-Methyl-1-naphthoyl chloride

Base Information

Chemical Name:6-Methyl-1-naphthoyl chloride
CAS No.:87700-71-8
Molecular Formula:C₁₂H₉ClO
Molecular Weight:204.656
Hs Code.:2916399090
DSSTox Substance ID:DTXSID60602221
Wikidata:Q82499191
Mol file:87700-71-8.mol

Synonyms:87700-71-8;6-methyl-1-naphthoyl chloride;1-Naphthalenecarbonyl chloride, 6-methyl- (9CI);SCHEMBL9228177;DTXSID60602221;TWEBOZKXUXHQEX-UHFFFAOYSA-N;6-Methylnaphthalene-1-carbonyl chloride;1-Naphthalenecarbonyl chloride,6-methyl-(9ci)

Suppliers and Price of 6-Methyl-1-naphthoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2-Methylnaphthalene-5-carbonylchloride
1g
$ 1836.65

Alichem
2-Methylnaphthalene-5-carbonylchloride
500mg
$ 1058.40

Total 3 raw suppliers

Chemical Property of 6-Methyl-1-naphthoyl chloride

Chemical Property:

Boiling Point:324.9±11.0 °C(Predicted)
PSA：17.07000
Density:1.231±0.06 g/cm3(Predicted)
LogP:3.52720
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:204.0341926
Heavy Atom Count:14
Complexity:226

Purity/Quality:: 2-Methylnaphthalene-5-carbonylchloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C(=CC=C2)C(=O)Cl

Technology Process of 6-Methyl-1-naphthoyl chloride

There total 2 articles about 6-Methyl-1-naphthoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 6315-19-1
6-methylnaphthalene-1-carboxylic acid

: 87700-71-8
6-methyl-1-naphthoyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In benzene; for 4h;
DOI:10.1021/ol047852e

Reference yield:

: 6315-19-1
6-methylnaphthalene-1-carboxylic acid

: 128104-54-1
5-bromo-2-naphthalenylmethyl bromide

: 87700-71-8
6-methyl-1-naphthoyl chloride

Guidance literature:: With thionyl chloride;

Reference yield:

: 87700-71-8
6-methyl-1-naphthoyl chloride

: S-7,7'-dimethyl-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / Et₃N / CH₂Cl₂; benzene; dimethylformamide

2: 80 percent / methyllithium / tetrahydrofuran; hexane / 15 h / -78 - 25 °C

3: 67 percent / air / 10 h / 185 °C

4: 79 percent / CuCl; (-)-sparteine / methanol; CH₂Cl₂ / 6 h / 25 °C / ultrasound

With air; methyllithium; triethylamine; copper(l) chloride; (-)-sparteine; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol047852e