(RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

Base Information

Chemical Name:(RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide
CAS No.:935732-18-6
Molecular Formula:C₂₄H₂₆OP₂S
Molecular Weight:424.483
Hs Code.:

Synonyms:(RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

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Chemical Property of (RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

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Technology Process of (RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

There total 1 articles about (RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 569680-61-1
(R)-1-phenyl-2-methylenephospholane-1-oxide

: 935732-36-8
(diphenylphosphinothioyl)-acetic acid tert-butyl ester

: 935732-18-6
(RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

Guidance literature:: (R)-1-phenyl-2-methylenephospholane-1-oxide; (diphenylphosphinothioyl)-acetic acid tert-butyl ester; With sodium hydride; In benzene; at 0 - 20 ℃; for 24.5h;

With formic acid; at 20 ℃;

With copper(I) oxide; In pyridine; for 12h; Heating / reflux;

Reference yield: 84.0%

: 935732-18-6
(RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide

: 935732-19-7
(RP,S)-cis-2-(2-diphenylphosphinoethyl)-1-phenylphospholane P,P-disulfide

Guidance literature:: (RP,S)-cis-2-[(2-diphenylthiophosphinoyl)ethyl]-1-phenylphospholane 1-oxide; With phenylsilane; In toluene; at 45 ℃; for 48h;

With sulfur; In benzene; at 20 ℃;