Technology Process of C14H22O4
There total 3 articles about C14H22O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / -20 °C / Inert atmosphere
2: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere
3: toluene-4-sulfonic acid / methanol / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; methanol; dichloromethane;
1: |Sharpless Asymmetric Epoxidation;
DOI:10.1016/j.tetlet.2012.07.043
DOI:10.1016/j.tetlet.2012.07.043
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / Inert atmosphere
2: toluene-4-sulfonic acid / methanol / Inert atmosphere
With
toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.07.043
DOI:10.1016/j.tetlet.2012.07.043