(2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

Base Information

Chemical Name:(2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate
CAS No.:959577-05-0
Molecular Formula:C₂₆H₃₂O₇
Molecular Weight:456.536
Hs Code.:

Synonyms:(2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

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Chemical Property of (2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

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Technology Process of (2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

There total 2 articles about (2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 17299-07-9
(2R,5R)-2,5-hexanediol

: 168170-58-9
(3’R,5’R-dibenzoyloxy-6’S-methyl-(2H)-tetrahydropyran-2-yloxy)-1-(2,2,2-trichloroacetimide)

: 959577-05-0
(2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1055/s-0029-1216967

Reference yield: 58.0%

: 17299-07-9
(2R,5R)-2,5-hexanediol

: 168393-80-4
(2S,3R,5R)-5-(benzoyloxy)-6-hydroxy-2-methyloxan-3-yl benzoate

: 959577-05-0
(2R,3R,5R,6S)-2-(((2R,5R)-5-hydroxyhexan-2-yl)oxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 2h; Molecular sieve;
DOI:10.1016/j.bmc.2013.07.018