(2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside

Base Information

• Chemical Name: (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside
• CAS No.: 1428421-67-3
• Molecular Formula: C₉₃H₁₄₅NO₁₀Si
• Molecular Weight: 1465.26
• Mol file: 1428421-67-3.mol

Synonyms:(2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside

Chemical Property of (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside

There total 1 articles about (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-hexacosanoic acid (506-46-7) + (2S,3S,4R,5S)-2-amino-3,4,5-tris(benzyloxy)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside (1428421-66-2) → (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside (1428421-67-3)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1016/j.carres.2013.01.010

Reference yield: 92.0%

(2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside (1428421-67-3) → (2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-α-D-galactopyranoside (1428421-68-4)

Guidance literature:

With pyridine; pyridine hydrofluoride; In tetrahydrofuran; at 20 ℃; for 0.833333h; Inert atmosphere;

DOI:10.1016/j.carres.2013.01.010

upstream raw materials:

1-hexacosanoic acid

(2S,3S,4R,5S)-2-amino-3,4,5-tris(benzyloxy)octadecyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-α-D-galactopyranoside

Downstream raw materials:

(2S,3S,4R,5S)-3,4,5-tris(benzyloxy)-2-(hexacosanoylamino)octadecyl 2,3-di-O-benzyl-α-D-galactopyranoside